MIL-P-514D (SUPPLEMENT 1)

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MIL-P-514D (SUPPLEMENT 1), MILITARY SPECIFICATION: PLATE, IDENTIFICATION, INSTRUCTION AND MARKING, BLANK (15 SEP 1966) [S/S BY A-A-50271].
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【英文标准名称】:StandardPracticeforHeatAgingofPlasticsWithoutLoad
【原文标准名称】:通用的玻璃制品齿轮油氧化和热稳定特性的标准实施规程
【标准号】:ASTMD3045-1992(2010)
【标准状态】:现行
【国别】:美国
【发布日期】:1992
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D20.50
【标准类型】:(Practice)
【标准水平】:()
【中文主题词】:
【英文主题词】:aging;exposure;heat;heat-aging;thermal-aging;Acceleratedaging/testing--plastics;Heataging;Heatingtests--plastics;Oxidationtesting--plastics;Thermalanalysis(TA)--plastics
【摘要】:Theuseofthispracticepresupposesthatthefailurecriteriaselectedtoevaluatematerials(thatis,thepropertyorpropertiesbeingmeasuredasafunctionofexposuretime)andthedurationoftheexposurecanbeshowntorelatetotheintendeduseofthematerials.Plasticmaterialsexposedtoheatmaybesubjecttomanytypesofphysicalandchemicalchanges.Theseverityoftheexposuresinbothtimeandtemperaturedeterminestheextentandtypeofchangethattakesplace.Aplasticmaterialisnotnecessarilydegradedbyexposuretoelevatedtemperatures,butmaybeunchangedorimproved.However,extendedperiodsofexposureofplasticstoelevatedtemperatureswillgenerallycausesomedegradation,withprogressivechangeinphysicalproperties.Generally,shortexposuresatelevatedtemperaturesmaydriveoutvolatilessuchasmoisture,solvents,orplasticizers,relievemoldingstresses,advancethecureofthermosets,andmaycausesomechangeincoloroftheplasticorcoloringagent,orboth.Normally,additionalshrinkageshouldbeexpectedwithlossofvolatilesoradvanceinpolymerization.Someplasticmaterialsmaybecomebrittleduetolossofplasticizersafterexposureatelevatedtemperatures.Othertypesofplasticsmaybecomesoftandsticky,eitherduetosorptionofvolatilizedplasticizerorduetobreakdownofthepolymer.Thedegreeofchangeobservedwilldependonthepropertymeasured.Differentproperties,mechanicalorelectrical,maynotchangeatthesamerate.Forinstance,thearcresistanceofthermosettingcompoundsimprovesuptothecarbonizationpointofthematerial.Mechanicalproperties,suchasflexuralproperties,aresensitivetoheatdegradationandmaychangeatamorerapidrate.Ultimatepropertiessuchasstrengthorelongationaremoresensitivetodegradationthanbulkpropertiessuchasmodulus,inmostcases.Effectsofexposuremaybequitevariable,especiallywhenspecimensareexposedforlongintervalsoftime.Factorsthataffectthereproducibilityofdataarethedegreeoftemperaturecontroloftheenclosure,humidityoftheoven,airvelocityoverthespecimen,andperiodofexposure.Errorsinexposurearecumulativewithtime.Certainmaterialsaresusceptibletodegradationduetotheinfluenceofhumidityinlong-termheatresistancetests.Materialssusceptibletohydrolysismayundergodegradationwhensubjectedtolong-termheatresistancetests.Itisnottobeinferredthatcomparativematerialrankingisundesirableorunworkable.Onthecontrary,thispracticeisdesignedtoprovidedatawhichcanbeusedforsuchcomparativepurposes.However,thedataobtainedfromthispractice,sinceitdoesnotaccountfortheinfluenceofstressorenvironmentthatisinvolvedinmostreallifeapplications,mustbeusedcautiouslybythedesigner,whomustinevitablymakematerialchoicesusingadditionaldatasuchascreepandcreeprupturethatareconsistentwiththerequirementsofhisspecificapplication.Itispossibleformanytemperatureindexestoexist,infact,oneforeachfailurecriterion.Therefore,foranyapplicationofthetemperatureindextobevalid,thethermalagingprogrammustduplicatetheintendedexposureconditionsoftheendproduct.Ifthematerialisstressedintheendproductinamannernotevaluatedintheagingprogram,thetemperatureindexthusderivedisnotapplicabletotheuseofthematerialinthatproduct.TherecanbeverylargeerrorswhenArrheniusplotsorequationsbasedondatafromexperimentsataseriesoftemperaturesareusedtoestimatetimetoproduceadefinedpropertychangeatsomelowertemperature.Thisestimateoftimetoproducethepropertychangeorx201C;failurex201D;atthelowertemperatureisoftencalledthex201C;
基本信息
标准名称:锡化学分析方法 铋量的测定
英文名称:Methods for chemical analysis of tin-Determination of bismuth content
中标分类: 冶金 >> 金属化学分析方法 >> 重金属极其合金分析方法
ICS分类: 冶金 >> 有色金属 >> 其他有色金属及其合金
替代情况:GB/T 3260.3-1982
发布部门:国家质量技术监督局
发布日期:2000-08-02
实施日期:2000-01-02
首发日期:1982-06-21
作废日期:1900-01-01
主管部门:中国有色金属工业协会
归口单位:全国有色金属标准化技术委员会
起草单位:云南锡业公司
出版社:中国标准出版社
出版日期:1900-01-01
页数:7页
适用范围

本标准规定了锡中铋含量的测定方法。本标准适用于锡中铋含量的测定。测定范围:0.00010%~0.080%。

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所属分类: 冶金 金属化学分析方法 重金属极其合金分析方法 冶金 有色金属 其他有色金属及其合金